Assuming you used the amounts for each reagents listed in the procedure and 215 mg of a
product was obtained and with an unexpected melting point of 76-77 o
C. Also, in the IR
spectrum obtain there were two strong peaks at 1515 cm-1 and 1310 cm-1
, which were not
seen in the starting material.
a. Write a complete lab report as per the post lab report guide detailed in the syllabus.
- Recrystallization was done in methanol. Can you give me a detail step by step procedure
for how you would have done this?